6R6Q
HIV capsid hexamer with IP5 ligand
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-03-03 |
Detector | OXFORD SAPPHIRE CCD |
Wavelength(s) | 0.978 |
Spacegroup name | P 6 |
Unit cell lengths | 90.693, 90.693, 56.958 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 78.000 - 2.730 |
R-factor | 0.22401 |
Rwork | 0.221 |
R-free | 0.28881 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6es8 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.445 |
Data reduction software | Adxv |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.000 | 2.790 |
High resolution limit [Å] | 2.730 | 2.730 |
Rmerge | 0.140 | 0.582 |
Number of reflections | 7234 | 956 |
<I/σ(I)> | 6.5 | |
Completeness [%] | 92.9 | 91 |
Redundancy | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 293 | PEG 6K, 0.1M NaCl |