6R6M
Kusta0087/Kusta0088 Complex purified from Kuenenia stuttgartiensis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-01-01 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 44.300, 130.360, 45.370 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.370 - 1.700 |
R-factor | 0.1895 |
Rwork | 0.188 |
R-free | 0.21030 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 0.972 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SHARP |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 63.000 | 1.800 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmeas | 0.060 | 0.610 |
Number of reflections | 29424 | 4287 |
<I/σ(I)> | 17.6 | 2.2 |
Completeness [%] | 98.8 | 93.4 |
Redundancy | 6.3 | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 293 | 20-25% PEG3000, 0.1 M Na-citrate |