6R3Z
Structure of the SBP FpvC in complex with Ni2+ ion from P. aeruginosa in P212121 space group
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-03-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 43.570, 62.690, 90.540 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.260 - 1.650 |
R-factor | 0.186 |
Rwork | 0.184 |
R-free | 0.21900 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | model soved by SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 0.970 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | FFT |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.260 | 1.750 |
High resolution limit [Å] | 1.650 | 1.650 |
Rpim | 0.051 | |
Number of reflections | 30063 | 4251 |
<I/σ(I)> | 12.8 | |
Completeness [%] | 97.8 | |
Redundancy | 10 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 292 | 16% PEG 6K, 0.1 M MES |