6R2M
Crystal structure of PssZ from Listeria monocytogenes
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-04-11 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97853 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.080, 71.560, 131.300 |
Unit cell angles | 90.00, 95.80, 90.00 |
Refinement procedure
Resolution | 43.540 - 1.617 |
R-factor | 0.1705 |
Rwork | 0.169 |
R-free | 0.19980 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 0.827 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.540 | 1.675 |
High resolution limit [Å] | 1.617 | 1.617 |
Number of reflections | 91306 | 8707 |
<I/σ(I)> | 59.37 | |
Completeness [%] | 94.6 | |
Redundancy | 10.6 | |
CC(1/2) | 0.806 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 7% PEG 400 (v/v), 24% PEG 5000 MME 0.1 M imidazole pH 7.0 |