6QZQ
Crystal structure of Csx1 from Sulfolobus islandicus monoclinic form
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-05-18 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 108.304, 119.579, 190.133 |
| Unit cell angles | 90.00, 106.25, 90.00 |
Refinement procedure
| Resolution | 72.550 - 3.600 |
| R-factor | 0.2033 |
| Rwork | 0.200 |
| R-free | 0.25710 |
| Structure solution method | SAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.959 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 72.550 | 3.790 |
| High resolution limit [Å] | 3.600 | 3.600 |
| Number of reflections | 49216 | 1279 |
| <I/σ(I)> | 11.2 | 2.9 |
| Completeness [%] | 99.5 | 90.7 |
| Redundancy | 7.9 | 6.8 |
| CC(1/2) | 0.990 | 0.870 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 0.1M Tris pH=8.5 8% PEG 8000 |
