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6QY6

Crystal structure of the CCA-adding enzyme of a psychrophilic organism

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSOLEIL BEAMLINE PROXIMA 1
Synchrotron siteSOLEIL
BeamlinePROXIMA 1
Temperature [K]100
Detector technologyPIXEL
Collection date2016-09-16
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.979
Spacegroup nameP 43 21 2
Unit cell lengths70.031, 70.031, 291.590
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution39.926 - 1.800
R-factor0.2083
Rwork0.207
R-free0.23210
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1miv
RMSD bond length0.007
RMSD bond angle0.794
Data reduction softwareXDS (20160617)
Data scaling softwareXSCALE (20160617)
Phasing softwarePHENIX (1.13_2998)
Refinement softwarePHENIX ((1.13_2998: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.910
High resolution limit [Å]1.8001.800
Rmeas0.0742.648
Number of reflections6855510787
<I/σ(I)>19.50.66
Completeness [%]99.999.3
Redundancy1312.9
CC(1/2)1.0000.590
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP293protein solution at 4.5 mg/mL in 50 mM Tris-HCl pH7.5, 200 mM NaCl, 5 mM MgCl2; reservoir solution: 100 mM Sodium acetate; pH 4.5 1 M di-Ammonium hydrogen phosphate

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