6QWZ

HEWL lysozyme, crystallized from KCl solution

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	KURCHATOV SNC BEAMLINE K4.4
Synchrotron site	KURCHATOV SNC
Beamline	K4.4
Temperature [K]	100
Detector technology	CCD
Collection date	2018-05-28
Detector	MAR CCD 165 mm
Wavelength(s)	0.80241
Spacegroup name	P 43 21 2
Unit cell lengths	78.660, 78.660, 37.061
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	27.810 - 1.350
R-factor	0.17042
Rwork	0.168
R-free	0.21647
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4wld
RMSD bond length	0.012
RMSD bond angle	1.585
Data reduction software	iMOSFLM
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	REFMAC (5.8.0135)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	27.810	1.385
High resolution limit [Å]	1.350	1.350
Rmerge	0.091
Number of reflections	26135
<I/σ(I)>	16.4
Completeness [%]	98.8
Redundancy	7.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	KCl