6QWQ
Structure of gtPebB
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-06-16 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 1.00601 |
| Spacegroup name | P 62 |
| Unit cell lengths | 109.600, 109.600, 47.980 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 47.458 - 1.900 |
| R-factor | 0.2121 |
| Rwork | 0.211 |
| R-free | 0.23280 |
| Structure solution method | SAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.777 |
| Data reduction software | XDS (BUILT=20160617) |
| Data scaling software | XSCALE (BUILT=20160617) |
| Phasing software | PHENIX (1.10.1_2155) |
| Refinement software | PHENIX ((dev_3126: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.458 | 1.968 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Number of reflections | 25797 | |
| <I/σ(I)> | 15.31 | |
| Completeness [%] | 98.7 | |
| Redundancy | 19 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 277 | 0.1 M Tris pH 8.5, 34.5 % PEG3350, 0.21 M ammonium sulfate |
