6QWO
Zinc-reconstituted ODP from T. maritima
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE F1 |
Synchrotron site | CHESS |
Beamline | F1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-06-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97900 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 46.433, 121.709, 159.531 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.220 - 2.000 |
Rwork | 0.165 |
R-free | 0.20930 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.220 | 2.071 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.126 | 0.656 |
Rmeas | 0.149 | 0.793 |
Rpim | 0.041 | 0.222 |
Number of reflections | 59080 | 3052 |
<I/σ(I)> | 7.5 | |
Completeness [%] | 99.8 | |
Redundancy | 10.7 | |
CC(1/2) | 0.992 | 0.887 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 30% polyethyleneglycol 1500 |