6QWO

Zinc-reconstituted ODP from T. maritima

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CHESS BEAMLINE F1
Synchrotron site	CHESS
Beamline	F1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-06-06
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97900
Spacegroup name	C 2 2 21
Unit cell lengths	46.433, 121.709, 159.531
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	23.220 - 2.000
Rwork	0.165
R-free	0.20930
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	23.220	2.071
High resolution limit [Å]	2.000	2.000
Rmerge	0.126	0.656
Rmeas	0.149	0.793
Rpim	0.041	0.222
Number of reflections	59080	3052
<I/σ(I)>	7.5
Completeness [%]	99.8
Redundancy	10.7
CC(1/2)	0.992	0.887

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		294	30% polyethyleneglycol 1500