6QVI
Crystal structure of competence-associated pilin ComZ from Thermus thermophilus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-02 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 1.0 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 121.860, 121.860, 212.350 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 58.790 - 2.720 |
R-factor | 0.209 |
Rwork | 0.206 |
R-free | 0.26700 |
Structure solution method | SAD |
RMSD bond length | 0.012 |
RMSD bond angle | 1.551 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | AutoSol |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 58.790 | 2.790 |
High resolution limit [Å] | 2.720 | 2.720 |
Rmerge | 0.058 | |
Number of reflections | 49699 | |
<I/σ(I)> | 18.1 | 2 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 5.8 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.2 M potassium thiocyanate, 0.1 M Bis-Tris propane pH 6.5 and 20% w/v PEG 3350 |