6QV7
Crystal structure of a CHAD domain from Chlorobium tepidum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-26 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.977948 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 69.483, 95.735, 102.779 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.805 - 1.720 |
R-factor | 0.1903 |
Rwork | 0.189 |
R-free | 0.22180 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3e0s |
RMSD bond length | 0.010 |
RMSD bond angle | 1.071 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 36.805 | 1.820 |
High resolution limit [Å] | 1.720 | 1.720 |
Rmeas | 0.074 | 2.210 |
Number of reflections | 70380 | 11411 |
<I/σ(I)> | 16.1 | 1 |
Completeness [%] | 100.0 | 99.8 |
Redundancy | 7 | 7.1 |
CC(1/2) | 1.000 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 2 M (NH4)2SO4, 5 % isopropanol |