6QPK
Zt-KP6-1: an effector from Zymoseptoria tritici
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-1 |
Synchrotron site | ESRF |
Beamline | MASSIF-1 |
Temperature [K] | 270 |
Detector technology | PIXEL |
Collection date | 2018-04-19 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.966 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 39.395, 57.294, 79.355 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.450 - 1.360 |
R-factor | 0.14 |
Rwork | 0.140 |
R-free | 0.18000 |
Structure solution method | SAD |
Data reduction software | XDS |
Data scaling software | Aimless (0.6.3) |
Phasing software | HKL2Map |
Refinement software | REFMAC (5.8.0222) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.450 | 1.400 |
High resolution limit [Å] | 1.360 | 1.360 |
Rmerge | 0.051 | |
Number of reflections | 448165 | 5272 |
<I/σ(I)> | 18.7 | 2.5 |
Completeness [%] | 91.3 | 56.7 |
Redundancy | 6.01 | 10.4 |
CC(1/2) | 0.450 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 298 | 0,1M Tris pH 9, 1.5M LiSO4 |