6QNM
Apo state of chemotaxis sensor ODP from T. denticola
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-06 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.979200 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.219, 94.800, 117.093 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.810 - 2.100 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.810 | 2.175 |
High resolution limit [Å] | 2.100 | 2.100 |
Number of reflections | 30165 | |
<I/σ(I)> | 4.6 | |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 6.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 0.1 M Imidazole pH 7.0, 20% PEG 4000 |