6QJD
Crystal Structure of the truncated form of the third PDZ domain of PSD-95: residues 302-392
Replaces: 5OHWExperimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-02-16 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.96864 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.118, 53.968, 62.613 |
Unit cell angles | 90.00, 93.25, 90.00 |
Refinement procedure
Resolution | 19.600 - 1.551 |
R-factor | 0.2183 |
Rwork | 0.216 |
R-free | 0.25900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3k82 |
Data scaling software | Aimless (0.3.11) |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.600 | 19.600 | 1.580 |
High resolution limit [Å] | 1.550 | 8.490 | 1.550 |
Rmerge | 0.144 | 0.126 | 0.487 |
Number of reflections | 48816 | 267 | 2452 |
<I/σ(I)> | 5.4 | ||
Completeness [%] | 94.1 | 80.9 | 96.7 |
Redundancy | 3.4 | 4.3 | 3.1 |
CC(1/2) | 0.983 | 0.980 | 0.729 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 298 | 0.2 M ammonium sulphate, 30% PEG 4000 |