6QJ2
Crystal structure of the C. thermophilum condensin Smc4 ATPase head in complex with the C-terminal domain of Brn1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-11-15 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 64 |
Unit cell lengths | 132.728, 132.728, 75.548 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.445 - 3.000 |
R-factor | 0.2153 |
Rwork | 0.214 |
R-free | 0.24300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1w1w |
Data reduction software | XDS |
Data scaling software | SCALA (3.3.22) |
Phasing software | PHENIX |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 114.946 | 45.741 | 3.060 |
High resolution limit [Å] | 2.900 | 9.170 | 2.900 |
Rmerge | 0.062 | 1.497 | |
Rmeas | 0.093 | 0.068 | 1.614 |
Rpim | 0.035 | 0.026 | 0.601 |
Number of reflections | 16953 | 568 | 2454 |
<I/σ(I)> | 12.4 | 9.1 | 0.5 |
Completeness [%] | 99.9 | 99 | 99.7 |
Redundancy | 6.9 | 6.4 | 7.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 3 % (v/v) EtOH, 0.1 M Na citrate pH 6.0, 1.5 M LiSO4 |