6QIZ
CI-2, conformation 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-10-21 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 6 2 2 |
Unit cell lengths | 68.550, 68.550, 53.099 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.580 - 1.650 |
R-factor | 0.186 |
Rwork | 0.184 |
R-free | 0.22000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ci2 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.862 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.580 | 1.710 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.083 | |
Number of reflections | 9305 | |
<I/σ(I)> | 15.2 | 1.6 |
Completeness [%] | 100.0 | 100 |
Redundancy | 8.3 | 8.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 25% PEG 3350, 100 MM TRIS-HCL PH 8.5 AND 200 MM LITHIUM SULPHATE, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 293K |