6QGL
Crystal structure of VP5 from Haloarchaeal pleomorphic virus 6
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-02-28 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.915 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 114.300, 114.300, 445.220 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 82.350 - 2.690 |
| R-factor | 0.219 |
| Rwork | 0.218 |
| R-free | 0.23300 |
| Structure solution method | SAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.990 |
| Data reduction software | xia2 |
| Data scaling software | xia2 |
| Phasing software | HKL2Map |
| Refinement software | BUSTER (2.10.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 90.450 | 2.760 |
| High resolution limit [Å] | 2.690 | 2.690 |
| Rmerge | 0.165 | 1.983 |
| Number of reflections | 49199 | 3541 |
| <I/σ(I)> | 17.4 | |
| Completeness [%] | 99.9 | 99.8 |
| Redundancy | 25.8 | 22.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | 1.6 M Ammonium Sulfate, 0.1 M Citrate pH 5.0 |
