6QEG
CRYSTAL STRUCTURE OF HUMAN METHIONINE AMINOPEPTIDASE-2 IN COMPLEX WITH AN INHIBITOR 2-Oxo-1-phenyl-pyrrolidine-3-carboxylic acid (2-thiophen-2-yl-ethyl)-amide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-17 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.54 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 89.265, 99.853, 100.417 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.080 - 2.080 |
R-factor | 0.18 |
Rwork | 0.178 |
R-free | 0.22800 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.080 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.7) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.080 | 2.150 |
High resolution limit [Å] | 2.080 | 2.080 |
Rmerge | 0.051 | 0.364 |
Number of reflections | 23388 | |
<I/σ(I)> | 11.4 | |
Completeness [%] | 85.5 | 79.1 |
Redundancy | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 277 | 20% METHANOL, 0.1 M CITRATE, PH 6.0 |