6Q4V
KlenTaq DNA polymerase in complex with dATP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-04-27 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9999 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 109.482, 109.482, 91.255 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.407 - 2.006 |
R-factor | 0.1874 |
Rwork | 0.186 |
R-free | 0.21860 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rtv |
RMSD bond length | 0.003 |
RMSD bond angle | 0.623 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((dev_3283: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.407 | 2.016 |
High resolution limit [Å] | 2.006 | 2.006 |
Rmeas | 0.076 | 1.082 |
Number of reflections | 81683 | 12970 |
<I/σ(I)> | 11.59 | 1.53 |
Completeness [%] | 99.6 | 97.8 |
Redundancy | 5.2 | 5.14 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291 | 27 % PEG 4000, 0.2 M ammonium acetate, 0.01 M magnesium (II) acetate, 0.1 M MES pH 6.5 |