6Q25
Coiled-coil Trimer with Glu:Leu:Lys Triad
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR591 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-09-29 |
Detector | APEX II CCD |
Wavelength(s) | 1.5406 |
Spacegroup name | H 3 |
Unit cell lengths | 39.063, 39.063, 101.522 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 17.409 - 1.893 |
R-factor | 0.1818 |
Rwork | 0.176 |
R-free | 0.22790 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | PROTEUM PLUS |
Data scaling software | PROTEUM PLUS |
Phasing software | PHENIX |
Refinement software | PHENIX (dev_2906) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 17.409 | 1.961 |
High resolution limit [Å] | 1.893 | 1.893 |
Rmerge | 0.191 | 0.532 |
Rmeas | 0.211 | 0.658 |
Rpim | 0.087 | 0.380 |
Number of reflections | 4584 | 469 |
<I/σ(I)> | 9.9 | 1.4 |
Completeness [%] | 98.9 | |
Redundancy | 4.9 | |
CC(1/2) | 0.948 | 0.668 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 298 | 50% PEG200, 100 mM HEPES free acid/NaOH, pH 7.5 |