6Q24
Structure of pro-Esp mutant- S235A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-06-25 |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 1.00 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 69.100, 69.100, 127.330 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.760 - 1.850 |
R-factor | 0.1951 |
Rwork | 0.193 |
R-free | 0.22190 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6pym |
RMSD bond length | 0.007 |
RMSD bond angle | 0.822 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.733 | 1.916 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.062 | 0.618 |
Rmeas | 0.088 | |
Number of reflections | 25463 | 2522 |
<I/σ(I)> | 8.76 | 1.22 |
Completeness [%] | 94.0 | |
Redundancy | 1.9 | |
CC(1/2) | 0.997 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Magnesium chloride, 0.1 M Sodium acetate pH 4.6, 30% PEG 4000 |