6PXB
N-Terminal SH2 domain of the p120RasGAP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-14 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9792 |
Spacegroup name | P 32 |
Unit cell lengths | 64.021, 64.021, 119.447 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.816 - 1.747 |
R-factor | 0.2221 |
Rwork | 0.220 |
R-free | 0.26300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4k44 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.810 |
High resolution limit [Å] | 1.747 | 3.770 | 1.750 |
Rmerge | 0.080 | 0.062 | 0.835 |
Rmeas | 0.084 | 0.065 | 0.890 |
Rpim | 0.026 | 0.020 | 0.303 |
Number of reflections | 55502 | 5536 | 5568 |
<I/σ(I)> | 5.4 | ||
Completeness [%] | 99.9 | 100 | 99.9 |
Redundancy | 9.9 | 10.4 | 8 |
CC(1/2) | 0.999 | 0.909 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 21% PEG 10,000 0.1M Tris pH 8.0 0.2M Ammonium Acetate |