6PRG
SBP RafE in complex with stachyose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-002 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-01-21 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.54187 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 49.278, 118.839, 146.012 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.940 - 2.350 |
R-factor | 0.2239 |
Rwork | 0.223 |
R-free | 0.24680 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2i58 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.677 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.390 |
High resolution limit [Å] | 2.350 | 2.350 |
Rmerge | 0.084 | 0.181 |
Rpim | 0.036 | 0.095 |
Number of reflections | 36605 | 3742 |
<I/σ(I)> | 20.2 | |
Completeness [%] | 99.9 | |
Redundancy | 5 | |
CC(1/2) | 0.995 | 0.966 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 291 | 0.2M CsCl, 0.1M Tris, 20% w/v PEG 3350 |