6PNY
X-ray Structure of Flpp3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | SLAC LCLS BEAMLINE CXI |
Synchrotron site | SLAC LCLS |
Beamline | CXI |
Temperature [K] | 300 |
Detector technology | PIXEL |
Collection date | 2015-04-02 |
Detector | CS-PAD CXI-1 |
Wavelength(s) | 1.425 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 28.000, 51.900, 68.100 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.000 - 1.650 |
R-factor | 0.1994 |
Rwork | 0.198 |
R-free | 0.23490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2mu4 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.584 |
Data reduction software | iMOSFLM |
Data scaling software | CrystFEL |
Phasing software | MR-Rosetta |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.000 | 1.710 |
High resolution limit [Å] | 1.650 | 1.650 |
Number of reflections | 16570 | 1143 |
<I/σ(I)> | 7.8 | |
Completeness [%] | 100.0 | |
Redundancy | 217 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | BATCH MODE | 300 | Sodium Chloride, Calcium Chloride, Sodium Phosphate |