6PL4
TRK-A IN COMPLEX WITH LIGAND 1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-10-27 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9999 |
Spacegroup name | P 31 1 2 |
Unit cell lengths | 52.052, 52.052, 227.917 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 45.078 - 2.060 |
R-factor | 0.20218 |
Rwork | 0.199 |
R-free | 0.23866 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.287 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 75.970 | 2.310 |
High resolution limit [Å] | 2.060 | 2.060 |
Rmerge | 0.040 | 0.443 |
Number of reflections | 21952 | |
<I/σ(I)> | 18.3 | |
Completeness [%] | 97.9 | 97.7 |
Redundancy | 2.9 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | pH 8.5 |