6PL4
TRK-A IN COMPLEX WITH LIGAND 1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-10-27 |
| Detector | DECTRIS PILATUS 6M-F |
| Wavelength(s) | 0.9999 |
| Spacegroup name | P 31 1 2 |
| Unit cell lengths | 52.052, 52.052, 227.917 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 45.078 - 2.060 |
| R-factor | 0.20218 |
| Rwork | 0.199 |
| R-free | 0.23866 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.287 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.970 | 2.310 |
| High resolution limit [Å] | 2.060 | 2.060 |
| Rmerge | 0.040 | 0.443 |
| Number of reflections | 21952 | |
| <I/σ(I)> | 18.3 | |
| Completeness [%] | 97.9 | 97.7 |
| Redundancy | 2.9 | 2.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277.15 | pH 8.5 |
