6PHH
Unliganded human transmission blocking antibody 2544
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-01 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97949 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 172.530, 43.650, 138.570 |
Unit cell angles | 90.00, 111.22, 90.00 |
Refinement procedure
Resolution | 38.976 - 2.400 |
R-factor | 0.2192 |
Rwork | 0.218 |
R-free | 0.24870 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | in house model |
RMSD bond length | 0.002 |
RMSD bond angle | 0.551 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.500 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.131 | 0.724 |
Rpim | 0.055 | 0.298 |
Number of reflections | 38316 | 4305 |
<I/σ(I)> | 11.2 | 1.6 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.7 | 6.9 |
CC(1/2) | 0.996 | 0.549 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 0.1 M sodium cacodylate HCl, pH 6.5, 1.0 M sodium citrate tribasic |