6PBU
ClpP1 from Mycobacterium smegmatis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-11-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 169.617, 169.617, 114.219 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.149 - 2.000 |
R-factor | 0.1795 |
Rwork | 0.178 |
R-free | 0.21460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2cby |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | BALBES |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.030 |
High resolution limit [Å] | 2.000 | 5.430 | 2.000 |
Rmerge | 0.122 | 0.035 | 1.181 |
Rmeas | 0.127 | 0.036 | 1.238 |
Rpim | 0.035 | 0.010 | 0.364 |
Total number of observations | 1387039 | ||
Number of reflections | 111562 | 5987 | 5412 |
<I/σ(I)> | 8.5 | ||
Completeness [%] | 99.7 | 99.7 | 98.3 |
Redundancy | 12.4 | 14.1 | 11 |
CC(1/2) | 1.000 | 0.813 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | 2.1 - 3.4 M sodium malonate pH 6.6 - 6.8 |