6PBB

Crystal structure of Hen Egg White Lysozyme in complex with I3C

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron site	Australian Synchrotron
Beamline	MX1
Temperature [K]	100
Detector technology	CCD
Collection date	2019-05-10
Detector	ADSC QUANTUM 210r
Wavelength(s)	1.4590
Spacegroup name	P 43 21 2
Unit cell lengths	77.160, 77.160, 38.201
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	34.507 - 1.892
R-factor	0.200725274419
Rwork	0.197
R-free	0.24034
Structure solution method	SAD
RMSD bond length	0.003
RMSD bond angle	0.539
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	Auto-Rickshaw
Refinement software	PHENIX (dev_2689)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	38.200	1.920
High resolution limit [Å]	1.870	1.870
Number of reflections	9810	475
<I/σ(I)>	23
Completeness [%]	98.4
Redundancy	43.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.1	289	0.2 M Ammonium acetate, 20% w/v Polyethylene glycol 3,350