6PAZ
OXIDIZED MUTANT P80I PSEUDOAZURIN FROM A. FAECALIS
Experimental procedure
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 298 |
Detector technology | AREA DETECTOR |
Collection date | 1994-04 |
Detector | SIEMENS |
Spacegroup name | P 65 |
Unit cell lengths | 50.790, 50.790, 98.250 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 18.260 - 1.910 |
R-factor | 0.175 * |
RMSD bond length | 0.005 |
RMSD bond angle | 0.016 |
Data reduction software | XENGEN |
Data scaling software | XENGEN |
Refinement software | SHELXL |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.260 | 2.000 |
High resolution limit [Å] | 1.910 | 1.910 |
Rmerge | 0.038 | 0.110 |
Number of reflections | 10151 | |
<I/σ(I)> | 20.4 | 3.4 |
Completeness [%] | 97.0 * | 80 * |
Redundancy | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.8 * | 50MM SODIUM PHOSPHATE WITH 75%, pH 7.0 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | protein | 20 (mg/ml) | |
2 | 1 | 1 | phosphate | 20 (mM) | |
3 | 1 | 1 | ammonium sulfate | 42 (%sat) |