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6P4Z

Structure of gadolinium-caged cobalt (III) insulin hexamer

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 24-ID-C
Synchrotron siteAPS
Beamline24-ID-C
Temperature [K]100
Detector technologyCCD
Collection date2015-04-11
DetectorADSC QUANTUM 315
Wavelength(s)0.979
Spacegroup nameH 3
Unit cell lengths81.400, 81.400, 33.700
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution23.498 - 1.800
R-factor0.1839
Rwork0.181
R-free0.23860
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.008
RMSD bond angle0.794
Data reduction softwareXDS
Data scaling softwareXDS
Phasing softwarePHASER
Refinement softwarePHENIX ((1.13_2998))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]23.5001.900
High resolution limit [Å]1.8001.800
Number of reflections72161153
<I/σ(I)>13.5
Completeness [%]92.9
Redundancy2.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP29318% (w/v) PEG 12,000 and 0.1 M HEPES pH 7.0

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