6P4I
Photoactive Yellow Protein PYP 10ps
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | FREE ELECTRON LASER |
Source details | EUROPEAN XFEL BEAMLINE SPB/SFX |
Synchrotron site | European XFEL |
Beamline | SPB/SFX |
Temperature [K] | 273 |
Detector technology | PIXEL |
Collection date | 2019-03-07 |
Detector | AGIPD |
Wavelength(s) | 1.3 |
Spacegroup name | P 63 |
Unit cell lengths | 66.900, 66.900, 40.800 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 11.150 - 1.600 |
R-factor | 0.28612 |
Rwork | 0.283 |
R-free | 0.34150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wl9 |
RMSD bond length | 0.020 |
RMSD bond angle | 2.236 |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | PHENIX |
Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 11.150 | 1.640 |
High resolution limit [Å] | 1.600 | 1.600 |
Number of reflections | 12253 | 685 |
<I/σ(I)> | 11.77 | |
Completeness [%] | 92.8 | |
Redundancy | 284.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 7 | 293 | Sodium Malonate |