6P39
Crystal Structure Analysis of TAF1 Bromodomain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-19 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9792 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 96.600, 96.600, 91.130 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 42.676 - 2.941 |
R-factor | 0.1936 |
Rwork | 0.193 |
R-free | 0.21230 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3uv5 |
Data reduction software | XDS |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.560 | 2.990 |
High resolution limit [Å] | 2.940 | 2.940 |
Rmeas | 0.092 | 1.928 |
Rpim | 0.030 | 0.599 |
Total number of observations | 104018 | 5346 |
Number of reflections | 10784 | 521 |
<I/σ(I)> | 15.8 | 1.4 |
Completeness [%] | 99.9 | 99.4 |
Redundancy | 9.6 | 10.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | PEG1000, Tris pH 8.0 |