6P0T
Crystal structure of ternary DNA complex "FX(1-2)-1Xis" containing E. coli Fis and phage lambda Xis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-03-07 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9793 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 108.190, 108.190, 152.580 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 88.255 - 3.603 |
R-factor | 0.2017 |
Rwork | 0.199 |
R-free | 0.24830 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6p0u |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.6.1) |
Refinement software | PHENIX ((1.15_3459)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 88.255 | 88.255 | 3.700 |
High resolution limit [Å] | 3.600 | 16.110 | 3.600 |
Rmerge | 0.118 | 0.055 | 0.816 |
Rmeas | 0.123 | 0.058 | 0.850 |
Total number of observations | 140007 | ||
Number of reflections | 10977 | 161 | 753 |
<I/σ(I)> | 13.14 | 29.94 | 3.09 |
Completeness [%] | 99.8 | 100 | 97.2 |
Redundancy | 12.755 | 10.193 | 12.697 |
CC(1/2) | 0.999 | 0.999 | 0.848 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 277 | 15% PEG 4000 |