6OZZ
N terminally deleted GapR crystal structure from C. crescentus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-16 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 43 2 2 |
Unit cell lengths | 106.410, 106.410, 139.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.703 - 3.304 |
R-factor | 0.2871 |
Rwork | 0.285 |
R-free | 0.32210 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.579 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.380 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.116 | 1.250 |
Number of reflections | 9555 | 49 |
<I/σ(I)> | 18 | 3.1 |
Completeness [%] | 76.1 | 5.4 |
Redundancy | 19.3 | 1.2 |
CC(1/2) | 0.999 | 0.880 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.4 | 295 | 4 % PEG 3350 0.16 M ammonium sulfate 0.6 % 1,2-butanediol |