6OZY
Wild type GapR crystal structure 2 from C. crescentus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-15 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9793 |
Spacegroup name | P 2 2 21 |
Unit cell lengths | 39.770, 59.370, 93.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.970 - 2.014 |
R-factor | 0.2352 |
Rwork | 0.233 |
R-free | 0.27260 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.002 |
RMSD bond angle | 0.428 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.970 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.095 | 0.808 |
Number of reflections | 10203 | 50 |
<I/σ(I)> | 16.5 | 3.1 |
Completeness [%] | 66.5 | 4.5 |
Redundancy | 8.5 | 0.5 |
CC(1/2) | 0.998 | 0.367 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.4 | 295 | 0.16 M ammonium sulfate 12 % PEG 3350 10 mM cadmium chloride |