6OWJ
Zn-mediated polymerization of human SFPQ
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-07-19 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.954 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 61.230, 62.450, 67.880 |
Unit cell angles | 90.00, 95.74, 90.00 |
Refinement procedure
Resolution | 27.380 - 1.940 |
R-factor | 0.178 |
Rwork | 0.176 |
R-free | 0.21800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4wii |
RMSD bond length | 0.010 |
RMSD bond angle | 1.030 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 27.380 | 1.990 |
High resolution limit [Å] | 1.940 | 1.940 |
Rmerge | 0.062 | 0.600 |
Rpim | 0.042 | 0.401 |
Number of reflections | 37507 | 2239 |
<I/σ(I)> | 10.3 | 1.6 |
Completeness [%] | 99.2 | |
Redundancy | 4.1 | |
CC(1/2) | 0.998 | 0.700 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 14% PEG4000, 0.2 M calcium chloride, 0.1 M MES, pH 6.0 |