6OVO
Crystal structure of the unliganded PG10 TCR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-09-29 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 61 |
Unit cell lengths | 149.620, 149.620, 55.991 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 44.826 - 2.490 |
R-factor | 0.179 |
Rwork | 0.177 |
R-free | 0.22160 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5wjo |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.14_3260) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 74.810 | 2.620 |
High resolution limit [Å] | 2.490 | 2.490 |
Rmerge | 0.148 | |
Rpim | 0.048 | 0.402 |
Number of reflections | 25252 | 2502 |
<I/σ(I)> | 11.2 | 2.2 |
Completeness [%] | 99.6 | 99.6 |
Redundancy | 10.2 | 7.6 |
CC(1/2) | 0.996 | 0.537 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, Ammonium Sulfate |