6OOP

protein B

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-B
Synchrotron site	APS
Beamline	23-ID-B
Temperature [K]	100
Detector technology	CCD
Collection date	2017-10-10
Detector	MAR CCD 130 mm
Wavelength(s)	1
Spacegroup name	C 1 2 1
Unit cell lengths	95.068, 63.149, 102.074
Unit cell angles	90.00, 100.87, 90.00

Refinement procedure

Resolution	15.000 - 2.800
Structure solution method	SAD
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	SHARP
Refinement software	REFMAC

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	15.000	2.900
High resolution limit [Å]	2.800	2.800
Number of reflections	12656	300
<I/σ(I)>	13
Completeness [%]	91.0
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	PEG 400