6ONB
Crystal Structure of the ZIG-8-RIG-5 IG1-IG1 heterodimer, monoclinic form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 120 |
Detector technology | PIXEL |
Collection date | 2019-02-27 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.97920 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 87.460, 79.103, 89.977 |
Unit cell angles | 90.00, 94.22, 90.00 |
Refinement procedure
Resolution | 89.733 - 1.696 |
R-factor | 0.1755 |
Rwork | 0.174 |
R-free | 0.20730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6on9 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.821 |
Data reduction software | XDS (20180808) |
Data scaling software | XDS (20180808) |
Phasing software | PHASER (2.8.3) |
Refinement software | PHENIX (1.15rc3_3435) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 1.800 |
High resolution limit [Å] | 1.696 | 1.700 |
Rmerge | 0.047 | 0.587 |
Rmeas | 0.055 | 0.692 |
Number of reflections | 65564 | 10243 |
<I/σ(I)> | 14.15 | 1.62 |
Completeness [%] | 96.8 | 93.8 |
Redundancy | 3.6 | 3.4 |
CC(1/2) | 0.999 | 0.812 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 295 | 0.2 M lithium sulfate, 0.1 M sodium cacodylate, pH 6.5, 30% PEG 400 |