Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRL BEAMLINE BL9-2 |
| Synchrotron site | SSRL |
| Beamline | BL9-2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2006-12-09 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.9794 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 56.640, 56.640, 195.930 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 28.310 - 1.600 |
| R-factor | 0.20639 |
| Rwork | 0.206 |
| R-free | 0.21724 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2hin |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.871 |
| Data reduction software | iMOSFLM |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0238) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.700 | 1.630 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmerge | 0.066 | 2.800 |
| Rpim | 0.019 | 1.700 |
| Number of reflections | 42733 | 1762 |
| <I/σ(I)> | 13.2 | 6.7 |
| Completeness [%] | 98.7 | 85.3 |
| Redundancy | 12.7 | 4.3 |
| CC(1/2) | 1.000 | 0.214 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.4 M ammonium phosphate monobasic |
