6OMO
Human BMP6 homodimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-12-16 |
Detector | MAC Science DIP-320 |
Wavelength(s) | 1.0 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 97.398, 97.398, 85.644 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.700 - 2.800 |
R-factor | 0.217 |
Rwork | 0.215 |
R-free | 0.24420 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.300 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | BUSTER (2.11.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 48.700 |
High resolution limit [Å] | 2.800 |
Number of reflections | 14720 |
<I/σ(I)> | 8 |
Completeness [%] | 99.5 |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100mM Tris HCl 8.0, 15% MPD |