Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2016-04-24 |
| Detector | MARMOSAIC 300 mm CCD |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 41 3 2 |
| Unit cell lengths | 228.116, 228.116, 228.116 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 24.889 - 3.850 |
| R-factor | 0.2226 |
| Rwork | 0.219 |
| R-free | 0.29660 |
| Structure solution method | SAD |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.702 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 25.000 | 4.220 |
| High resolution limit [Å] | 3.850 | 3.850 |
| Rpim | 0.076 | 0.727 |
| Number of reflections | 19830 | 4618 |
| <I/σ(I)> | 7.6 | |
| Completeness [%] | 99.6 | |
| Redundancy | 9.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 295 | 32% PEG400, 0.05 M sodium acetate, 0.1 M magnesium acetate, 3.6 mM decyl beta-D-maltoside |
