6OI4
RPN13 (19-132)-RPN2 (940-952) pY950-Ub complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2016-12-12 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 |
Unit cell lengths | 99.373, 99.373, 41.705 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 29.947 - 1.760 |
R-factor | 0.1743 |
Rwork | 0.173 |
R-free | 0.20710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5v1y |
RMSD bond length | 0.011 |
RMSD bond angle | 1.157 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.820 |
High resolution limit [Å] | 1.760 | 1.760 |
Rpim | 0.069 | 0.663 |
Number of reflections | 46327 | 4392 |
<I/σ(I)> | 12.8 | |
Completeness [%] | 99.0 | 98 |
Redundancy | 9.2 | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.8 | 277 | 0.1 M citric acid, pH 4.6, 20% PEG6000 |