6OHU
Structure of EBP and tamoxifen
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-11-16 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0,979 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 192.837, 66.829, 98.678 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.799 - 3.526 |
R-factor | 0.2778 |
Rwork | 0.273 |
R-free | 0.32590 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 0.927 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.570 |
High resolution limit [Å] | 3.500 | 3.500 |
Number of reflections | 13685 | 821 |
<I/σ(I)> | 17.3 | |
Completeness [%] | 99.6 | |
Redundancy | 6.3 | |
CC(1/2) | 0.950 | 0.358 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | Hepes, peg 600 |