6OHL
Crystal structure of Fusobacterium nucleatum flavodoxin bound to flavin mononucleotide
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2018-09-13 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.5418 |
Spacegroup name | H 3 2 |
Unit cell lengths | 118.872, 118.872, 103.375 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 25.066 - 1.850 |
R-factor | 0.1695 |
Rwork | 0.168 |
R-free | 0.19120 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.024 |
Data reduction software | DENZO |
Data scaling software | HKL-2000 |
Phasing software | PHASER (2.7.16) |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 1.880 |
High resolution limit [Å] | 1.850 | 5.020 | 1.850 |
Rmerge | 0.092 | 0.037 | 0.492 |
Rmeas | 0.097 | 0.038 | 0.556 |
Rpim | 0.030 | 0.012 | 0.251 |
Total number of observations | 235021 | ||
Number of reflections | 23672 | 1267 | 912 |
<I/σ(I)> | 6.3 | ||
Completeness [%] | 98.3 | 99.1 | 76.6 |
Redundancy | 9.9 | 10.6 | 3.8 |
CC(1/2) | 0.999 | 0.789 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 42-46% PEG 600, 0.16-0.18 M calcium acetate, 0.1 M sodium cacodylate |