6OD1
IraD-bound to RssB D58P variant
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 55.938, 55.938, 300.298 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.080 - 2.000 |
R-factor | 0.2025 |
Rwork | 0.200 |
R-free | 0.24500 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 0.938 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.14_3260: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.100 | 2.100 |
High resolution limit [Å] | 2.000 | 2.050 |
Number of reflections | 3053 | 5272 |
<I/σ(I)> | 25 | |
Completeness [%] | 96.9 | |
Redundancy | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | magnesium chloride, PEG 8000, Tris pH 8.5 |