6OAV
JAK2 JH2 in complex with JAK146
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-25 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 44.123, 57.356, 60.744 |
Unit cell angles | 90.00, 110.45, 90.00 |
Refinement procedure
Resolution | 41.343 - 1.939 |
R-factor | 0.2019 |
Rwork | 0.200 |
R-free | 0.23600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5usz |
RMSD bond length | 0.007 |
RMSD bond angle | 0.775 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 200.000 | 2.060 |
High resolution limit [Å] | 1.939 | 1.940 |
Rmeas | 0.113 | |
Number of reflections | 20958 | 3430 |
<I/σ(I)> | 11.7 | |
Completeness [%] | 98.6 | |
Redundancy | 5.9 | |
CC(1/2) | 0.867 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 277.15 | 0.1M TRIS, PH 8.0 0.2M SODIUM ACETATE, 0.001 M TCEP, 12-24% PEG 4,000 |