6OAK
Structure of human PARG complexed with JA2131
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-12-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.497, 89.333, 94.161 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.078 - 1.700 |
R-factor | 0.1835 |
Rwork | 0.182 |
R-free | 0.20880 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4b1g |
RMSD bond length | 0.004 |
RMSD bond angle | 0.799 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.078 | 1.761 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.139 | 2.688 |
Number of reflections | 62296 | 6098 |
<I/σ(I)> | 17.71 | |
Completeness [%] | 100.0 | 99 |
Redundancy | 19.1 | 13.1 |
CC(1/2) | 0.999 | 0.431 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 295 | 0.1 M PCTP, pH 7.5, 0.2 M (NH3)2SO4, 17% PEG3350 |