6O8Q
HUaa 19bp SYM DNA pH 4.5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-29 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.115830 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.411, 61.151, 351.203 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.180 - 3.216 |
R-factor | 0.2504 |
Rwork | 0.247 |
R-free | 0.28540 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.692 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.180 | 3.331 |
High resolution limit [Å] | 3.216 | 3.216 |
Rmerge | 0.177 | 1.388 |
Rmeas | 0.185 | 1.444 |
Rpim | 0.053 | |
Number of reflections | 20484 | 1608 |
<I/σ(I)> | 11.31 | |
Completeness [%] | 93.9 | 73.05 |
Redundancy | 12.3 | |
CC(1/2) | 0.999 | 0.830 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4 | 293.15 | 0.1 M Na-malonate, pH 4.0 12% PEG 3350 |