6O6M
The Structure of EgtB (Cabther)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.3 |
Synchrotron site | ALS |
Beamline | 5.0.3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-09-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97648 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 85.294, 137.315, 85.391 |
Unit cell angles | 90.00, 92.43, 90.00 |
Refinement procedure
Resolution | 45.855 - 2.506 |
R-factor | 0.1865 |
Rwork | 0.185 |
R-free | 0.22570 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.656 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.860 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Number of reflections | 67215 | 4473 |
<I/σ(I)> | 7.5 | |
Completeness [%] | 100.0 | |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | 0.1M Na acetate 0.1M Tris acetate 5% PEG 4000 |